Agradecimentos: The authors would like to acknowledge the financial support of Colciencias by the scholarship No. 512 from 2010. We would like to thank the following institutions: Petrobras and LNNano/CNPEM for providing economic funding and laboratory facilities where this work was developed;...

Agradecimentos: The authors would like to acknowledge the financial support of Colciencias by the scholarship No. 512 from 2010. We would like to thank the following institutions: Petrobras and LNNano/CNPEM for providing economic funding and laboratory facilities where this work was developed; TenarisConfab for the materials donation. Vinicius Lima is thanked for his enormous collaboration with the CTOD testing during the course of the work. Special thanks is due to David Read for his important review and suggestions of the document

Friction stir welding with the optimum parameters offers high toughness and mechanical properties for pipeline steel applications; however, at subzero temperatures such joints have shown decreased toughness relative to room temperatures values as well as predominantly brittle behavior. This paper...

Friction stir welding with the optimum parameters offers high toughness and mechanical properties for pipeline steel applications; however, at subzero temperatures such joints have shown decreased toughness relative to room temperatures values as well as predominantly brittle behavior. This paper relates certain microstructural features to fracture toughness for the different regions of one- and two-pass friction stir welded joints, including base material, heat-affected, stir and hard zones. Toughness was assessed at 0 °C, −20 °C and −40 °C by crack tip opening displacement testing. The microstructures in the stir and hard zones were composed mainly of granular bainite, and bainite packets with irregular and straight ferrite plates. Hardness mapping distinguished the hard zone from the base material and stir zone, and from the heat affected zone that undergoes a softening relative to base material. The effects of low temperatures on the toughness were more pronounced in notches located at the stir zone and hard zone than for other notches. Detailed SEM fractography revealed the complementary roles of martensite-austenite particles, and bainite packets in the initiation and propagation of cleavage fracture in the hard zone at −40 °C

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